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LABOMATIC Instruments pump: labomatic hd-5000 or hd-3000
Pump: Labomatic Hd 5000 Or Hd 3000, supplied by LABOMATIC Instruments, used in various techniques. Bioz Stars score: 90/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
https://www.bioz.com/product/pump%3A+labomatic+hd-5000+or+hd-3000/hplc+gradient+pump+labomatic+hd+3000/us12152041-725-7-27
Average 90 stars, based on 1 article reviews
pump: labomatic hd-5000 or hd-3000 - by Bioz Stars, 2026-10
90/100 stars

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Injection:

Article Title: Macrocyclic indole derivatives
Article Snippet: Method P6: Instrument: Pump: Labomatic HD-5000 or HD-3000, Head HDK 280, low pressure gradient module ND-B1000; Manual injection valve: Rheodyne 3725i038; Detector: Knauer Azura UVD 2.15; Collector: Labomatic Labocol Vario-4000; Column: Chromatorex RP C-18 10 μm, 125×30 mm; Solvent A: water+0.1 Vol-% formic acid (32%), Solvent B: acetonitrile, Gradient: 0.00-0.50 min 20% B (150 ml/min), 0.50-6.00 min 20-90% B (150 mL/min), 6.00-6.10 min 90-100% B (150 mL/min), 6.10-8.00 min 100% B (150 mL/min), UV-Detection.

Article Title: Macrocyclic indole derivatives
Article Snippet: Method P5: Instrument: Pump: Labomatic HD-5000 or HD-3000, Head HDK 280, low pressure gradient module ND-B1000; Manual injection valve: Rheodyne 3725i038; Detector: Knauer Azura UVD 2.15; Collector: Labomatic Labocol Vario-4000; Column: Chromatorex RP C-18 10 μm, 125×30 mm; Solvent A: water+0.1 Vol-% formic acid (32%), Solvent B: acetonitrile, Gradient: 0.00-0.50 min 35% B (150 ml/min), 0.50-6.00 min 35-100% B (150 mL/min), 6.00-8.00 min 100% B (150 mL/min), UV-Detection.

Article Title: Macrocyclic indole derivatives
Article Snippet: Analytical UPLC Methods: Method 1: Instrument: Waters Acquity UPLCMS SingleQuad; Column: Acquity UPLC BEH C18 1.7 μm, 50×2.1 mm; eluent A: water+0.1 vol % formic acid (99%), eluent B: acetonitrile; gradient: 0-1.6 min 1-99% B, 1.6-2.0 min 99% B; flow 0.8 ml/min; temperature: 60° C.; DAD scan: 210-400 nm.

Article Title: Macrocyclic indole derivatives
Article Snippet: Method P4: Instrument: Pump: Labomatic HD-5000 or HD-3000, Head HDK 280, low pressure gradient module ND-B1000; Manual injection valve: Rheodyne 3725i038; Detector: Knauer Azura UVD 2.15; Collector: Labomatic Labocol Vario-4000; Column: Chromatorex RP C-18 10 μm, 125×30 mm; Solvent A: water+0.1 Vol-% formic acid (32%), Solvent B: acetonitrile, Gradient: 0.00-0.50 min 30% B (150 ml/min), 0.50-6.00 min 30-70% B (150 mL/min), 6.00-6.10 min 70-100% B (150 mL/min), 6.10-8.00 min 100% B (150 mL/min), UV-Detection.

Article Title: Macrocyclic indole derivatives
Article Snippet: Method 4: Instrument: Waters Acquity UPLCMS SingleQuad; Column: Acquity UPLC BEH C18 1.7 μm, 50×2.1 mm; eluent A: water+0.2 vol % aqueous ammonia (32%), eluent B: acetonitrile; gradient: 0-1.6 min 1-99% B, 1.6-2.0 min 99% B; flow 0.8 ml/min; temperature: 60° C.; DAD scan: 210-400 nm Preparative HPLC Methods: Method P1: Instrument: Waters Autopurification MS SingleQuad; Column: Waters XBrigde C18 5μ 100×30 mm; eluent A: water+0.1 vol % formic acid (99%), eluent B: acetonitrile; gradient: 0-5.5 min 5-100% B; flow 70 ml/min; temperature: 25° C.; DAD scan: 210-400 nm.

Article Title: Macrocyclic indole derivatives
Article Snippet: Method P2: Instrument: Waters Autopurification MS SingleQuad; Column: Waters XBrigde C18 5μ 100×30 mm; eluent A: water+0.2 vol % aqueous ammonia (32%), eluent B: acetonitrile; gradient: 0-5.5 min 5-100% B; flow 70 ml/min; temperature: 25° C.; DAD scan: 210-400 nm.

Article Title: Macrocyclic indole derivatives
Article Snippet: Method P8: Instrument: Pump: Labomatic HD-5000 or HD-3000, Head HDK 280, low pressure gradient module ND-B1000; Manual injection valve: Rheodyne 3725i038; Detector: Knauer Azura UVD 2.15; Collector: Labomatic Labocol Vario-4000; Column: XBridge, RP C18 5 μm, 100×30 mm; Solvent A: water+0.2 Vol-% ammonia (32%), Solvent B: acetonitrile, gradient: 0.00-2.00 min 10% B (60 ml/min), 2.00-14.00 min 10-50% B (60 ml/min), 14.00-14.10 min 50-100% B (60 ml/min), 14.10-17.00 min 100% B (60 ml/min), UV-Detection.

Article Title: Substituted macrocyclic indole derivatives
Article Snippet: Method 9: MS instrument type: Shimadzu LCMS-2020; HPLC instrument type: Shimadzu UV SPD-M20A; column: Kinetex EVO C18 2.1*30 mm*5 um; mobile phase A: 0.025% NH3·H2O in water (v/v), mobile phase B: acetonitrile; gradient: 0.00 min 5% B—0.80 min 95% B—1.2 min 95% B—1.21 min 5% B—1.5 min 5% B; flow rate: 1.5 mL/min; Column Temp: 40° C.; UV detection: 220 nm & 254 nm.

Solvent:

Article Title: Macrocyclic indole derivatives
Article Snippet: Method P6: Instrument: Pump: Labomatic HD-5000 or HD-3000, Head HDK 280, low pressure gradient module ND-B1000; Manual injection valve: Rheodyne 3725i038; Detector: Knauer Azura UVD 2.15; Collector: Labomatic Labocol Vario-4000; Column: Chromatorex RP C-18 10 μm, 125×30 mm; Solvent A: water+0.1 Vol-% formic acid (32%), Solvent B: acetonitrile, Gradient: 0.00-0.50 min 20% B (150 ml/min), 0.50-6.00 min 20-90% B (150 mL/min), 6.00-6.10 min 90-100% B (150 mL/min), 6.10-8.00 min 100% B (150 mL/min), UV-Detection.

Article Title: Macrocyclic indole derivatives
Article Snippet: Method P5: Instrument: Pump: Labomatic HD-5000 or HD-3000, Head HDK 280, low pressure gradient module ND-B1000; Manual injection valve: Rheodyne 3725i038; Detector: Knauer Azura UVD 2.15; Collector: Labomatic Labocol Vario-4000; Column: Chromatorex RP C-18 10 μm, 125×30 mm; Solvent A: water+0.1 Vol-% formic acid (32%), Solvent B: acetonitrile, Gradient: 0.00-0.50 min 35% B (150 ml/min), 0.50-6.00 min 35-100% B (150 mL/min), 6.00-8.00 min 100% B (150 mL/min), UV-Detection.

Article Title: Macrocyclic indole derivatives
Article Snippet: Analytical UPLC Methods: Method 1: Instrument: Waters Acquity UPLCMS SingleQuad; Column: Acquity UPLC BEH C18 1.7 μm, 50×2.1 mm; eluent A: water+0.1 vol % formic acid (99%), eluent B: acetonitrile; gradient: 0-1.6 min 1-99% B, 1.6-2.0 min 99% B; flow 0.8 ml/min; temperature: 60° C.; DAD scan: 210-400 nm.

Article Title: Macrocyclic indole derivatives
Article Snippet: Method P4: Instrument: Pump: Labomatic HD-5000 or HD-3000, Head HDK 280, low pressure gradient module ND-B1000; Manual injection valve: Rheodyne 3725i038; Detector: Knauer Azura UVD 2.15; Collector: Labomatic Labocol Vario-4000; Column: Chromatorex RP C-18 10 μm, 125×30 mm; Solvent A: water+0.1 Vol-% formic acid (32%), Solvent B: acetonitrile, Gradient: 0.00-0.50 min 30% B (150 ml/min), 0.50-6.00 min 30-70% B (150 mL/min), 6.00-6.10 min 70-100% B (150 mL/min), 6.10-8.00 min 100% B (150 mL/min), UV-Detection.

Article Title: Macrocyclic indole derivatives
Article Snippet: Method 4: Instrument: Waters Acquity UPLCMS SingleQuad; Column: Acquity UPLC BEH C18 1.7 μm, 50×2.1 mm; eluent A: water+0.2 vol % aqueous ammonia (32%), eluent B: acetonitrile; gradient: 0-1.6 min 1-99% B, 1.6-2.0 min 99% B; flow 0.8 ml/min; temperature: 60° C.; DAD scan: 210-400 nm Preparative HPLC Methods: Method P1: Instrument: Waters Autopurification MS SingleQuad; Column: Waters XBrigde C18 5μ 100×30 mm; eluent A: water+0.1 vol % formic acid (99%), eluent B: acetonitrile; gradient: 0-5.5 min 5-100% B; flow 70 ml/min; temperature: 25° C.; DAD scan: 210-400 nm.

Article Title: Macrocyclic indole derivatives
Article Snippet: Method P2: Instrument: Waters Autopurification MS SingleQuad; Column: Waters XBrigde C18 5μ 100×30 mm; eluent A: water+0.2 vol % aqueous ammonia (32%), eluent B: acetonitrile; gradient: 0-5.5 min 5-100% B; flow 70 ml/min; temperature: 25° C.; DAD scan: 210-400 nm.

Article Title: Macrocyclic indole derivatives
Article Snippet: Method P8: Instrument: Pump: Labomatic HD-5000 or HD-3000, Head HDK 280, low pressure gradient module ND-B1000; Manual injection valve: Rheodyne 3725i038; Detector: Knauer Azura UVD 2.15; Collector: Labomatic Labocol Vario-4000; Column: XBridge, RP C18 5 μm, 100×30 mm; Solvent A: water+0.2 Vol-% ammonia (32%), Solvent B: acetonitrile, gradient: 0.00-2.00 min 10% B (60 ml/min), 2.00-14.00 min 10-50% B (60 ml/min), 14.00-14.10 min 50-100% B (60 ml/min), 14.10-17.00 min 100% B (60 ml/min), UV-Detection.

Article Title: Substituted macrocyclic indole derivatives
Article Snippet: Method 9: MS instrument type: Shimadzu LCMS-2020; HPLC instrument type: Shimadzu UV SPD-M20A; column: Kinetex EVO C18 2.1*30 mm*5 um; mobile phase A: 0.025% NH3·H2O in water (v/v), mobile phase B: acetonitrile; gradient: 0.00 min 5% B—0.80 min 95% B—1.2 min 95% B—1.21 min 5% B—1.5 min 5% B; flow rate: 1.5 mL/min; Column Temp: 40° C.; UV detection: 220 nm & 254 nm.



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